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Get Free AccessFully unsubstituted 4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (BODIPY) 1 was prepared. Reaction of 8-thiomethylbodipy 2 with triethylsilane in the presence of a catalytic amount of Pd and a stoichiometric amount of copper(I) thienyl-2-carboxylate (CuTC) in THF at 55 degrees C gave compound 1 in nearly quantitative yield. This compound displays high quantum yields (up to 93%) in polar solvents including water. Its optical properties and crystal structure are discussed.
Ismael J. Arroyo‐Córdoba, Rongrong Hu, Gabriel Merino, Ben Zhong Tang, Eduardo Peña‐Cabrera (2009). The Smallest and One of the Brightest. Efficient Preparation and Optical Description of the Parent Borondipyrromethene System. , 74(15), DOI: https://doi.org/10.1021/jo901014w.
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Type
Article
Year
2009
Authors
5
Datasets
0
Total Files
0
Language
en
DOI
https://doi.org/10.1021/jo901014w
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