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Get Free AccessA quasi in situ method using a specially developed holder is presented to follow electrochemically induced microstructural changes on a nanometre scale using analytical transmission electron microscopy (TEM). By following a specific specimen area after repeated exposure to oxygen bubbled through aqueous HCl of pH=3, de-alloying of a grain-boundary precipitate of ∼200nm was observed by monitoring the changes in the EELS copper L2,3-edge and EFTEM elemental maps. These results, supporting the existing models of de-alloying of copper rich precipitates in aluminium alloys, demonstrate the effectiveness of the quasi in situ specimen holder for analytical TEM studies of corrosion.
Sairam K. Malladi, F.D. Tichelaar, Qiang Xu, Minxian Wu, Herman Terryn, J.M.C. Mol, F. Hannour, H.W. Zandbergen (2012). Quasi in situ analytical TEM to investigate electrochemically induced microstructural changes in alloys: AA2024-T3 as an example. Corrosion Science, 69, pp. 221-225, DOI: 10.1016/j.corsci.2012.12.006.
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Type
Article
Year
2012
Authors
8
Datasets
0
Total Files
0
Language
English
Journal
Corrosion Science
DOI
10.1016/j.corsci.2012.12.006
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