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Get Free AccessOperando odd random phase electrochemical impedance spectroscopy (ORP-EIS) is introduced as an in-situ monitoring tool to directly monitor the conversion treatment of a zinc substrate in a hybrid Zr-based solution containing aminosilane and Cu additives. SEM and EDX are applied to investigate the morphology and elemental composition of the oxide film. Results show that the operando ORP-EIS provides an opportunity to investigate the growth of the conversion layer and its surface homogeneity during conversion. Moreover, operando ORP-EIS data reveal that the presence of aminosilane in the Zr solution containing Cu, improves the morphology and barrier properties of the conversion film.
Meisam Dabiri Havigh, Mohaddese Nabizadeh, Benny Wouters, Noël Hallemans, Tom Hauffman, John Lataire, Annick Hubin, Herman Terryn (2023). Operando Odd Random Phase Electrochemical Impedance Spectroscopy (Orp-Eis) for in Situ Monitoring of the Zr-Based Conversion Coating Growth in the Presence of (In)Organic Additives. , DOI: 10.2139/ssrn.4468382.
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Type
Preprint
Year
2023
Authors
8
Datasets
0
Total Files
0
Language
English
DOI
10.2139/ssrn.4468382
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