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Get Free AccessPalladium on magnesium oxide is able to allow a one‐pot reaction to synthesize thioethers from thiols and aldehydes formed in situ from the respective alcohol by means of a borrowing hydrogen method. The reaction is initiated by dehydrogenation of the alcohol to give a palladium hydride intermediate and an aldehyde. The latter reacts with a thiol involving most probably the intermediacy of a thionium ion RCHS + R, which can be reduced in situ by the metal hydride to afford thioethers.
Avelino Avelino, Javier Navas, Tania Ródenas, María J. Sabater (2013). One‐Pot Palladium‐Catalyzed Borrowing Hydrogen Synthesis of Thioethers. Chemistry - A European Journal, 19(51), pp. 17464-17471, DOI: 10.1002/chem.201302226.
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Type
Article
Year
2013
Authors
4
Datasets
0
Total Files
0
Language
English
Journal
Chemistry - A European Journal
DOI
10.1002/chem.201302226
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