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Get Free AccessIt was found that either polymorph B or polymorph C of zeolite beta can be obtained from the same structure directing agent: 4,4-dimethyl-4-azonia-tricyclo[5.2.2.02,6]undec-8-ene hydroxide. The synthesis occurs through a consecutive process where polymorph B is first formed and then transformed into polymorph C. It is possible to produce a zeolite highly enriched in polymorph B, provided that the transformation of this phase into polymorph C is slowed down up to the point where polymorph C is only detected at trace levels. The structure of polymorph B was determined for the first time by electron crystallography with SAED and HRTEM from areas of unfaulted polymorph B crystals.
Avelino Avelino, Manuel Moliner, Ángel Cantı́n, María J. Díaz‐Cabañas, J.L. Jordá, Daliang Zhang, Junliang Sun, Kjell Jansson, Sven Hovmöller, Xiaodong Zou (2008). Synthesis and Structure of Polymorph B of Zeolite Beta. Chemistry of Materials, 20(9), pp. 3218-3223, DOI: 10.1021/cm8002244.
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Type
Article
Year
2008
Authors
10
Datasets
0
Total Files
0
Language
English
Journal
Chemistry of Materials
DOI
10.1021/cm8002244
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