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Get Free AccessThe porous organosilica framework containing Tröger's base (TB) prepared by mild sol–gel synthesis from 2,8-bis-silylated TB precursor contains a mixture of two point attached TB and one point attached TB units, resulting from unexpected partial Si–C bond cleavage as demonstrated by 29Si MAS NMR spectroscopy and by selective chemo-desorption of the anchored organic part of the hybrid material.
Evelyne Poli, Estı́baliz Merino, Urbano Díaz, Daniel Brunel, Avelino Avelino (2011). Si–C attachment points during sol–gel synthesis of organosilicas from 2,8-bis-silylated Tröger's base as building block precursor. Journal of Materials Chemistry, 21(24), pp. 8524-8524, DOI: 10.1039/c1jm10426h.
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Type
Article
Year
2011
Authors
5
Datasets
0
Total Files
0
Language
English
Journal
Journal of Materials Chemistry
DOI
10.1039/c1jm10426h
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