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  5. From Well-Defined Clusters to Functional Materials: Molecular Engineering of Amorphous Molybdenum Sulfides for Hydrogen Evolution Electrocatalysis

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Article
English
2023

From Well-Defined Clusters to Functional Materials: Molecular Engineering of Amorphous Molybdenum Sulfides for Hydrogen Evolution Electrocatalysis

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English
2023
Chemistry of Materials
Vol 35 (20)
DOI: 10.1021/acs.chemmater.3c01260

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Avelino Avelino
Avelino Avelino

Instituto de Tecnología Química

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Francisco Gonell
Miriam Rodenes
Santiago Martı́n
+3 more

Abstract

Developing precious-metal-free electrocatalysts for the hydrogen evolution reaction (HER) is crucial to establishing H2 produced from renewable energy sources as an alternative energy carrier to fossil fuels. Amorphous molybdenum sulfide-based materials are promising candidates that provide highly active HER electrocatalysts by introducing active sites at both the edge positions and the typically inactive basal planes. Herein, we report an innovative bottom-up synthesis of amorphous molybdenum sulfides using molecular complexes with Mo3S4 and Mo3S7 cluster cores as building entities. The ability to control the precursor of choice has made it viable to enhance the HER activity of these materials. Furthermore, the tunability of the atomic composition of the molecular cluster precursors allows the modification of the derived materials with atomic-scale precision, enabling us to track the synthesis mechanism and, in combination with Density Functional Theory (DFT) calculations, to decipher the nature of the HER active sites.

How to cite this publication

Francisco Gonell, Miriam Rodenes, Santiago Martı́n, Mercedes Boronat, Iván Sorribes, Avelino Avelino (2023). From Well-Defined Clusters to Functional Materials: Molecular Engineering of Amorphous Molybdenum Sulfides for Hydrogen Evolution Electrocatalysis. Chemistry of Materials, 35(20), pp. 8483-8493, DOI: 10.1021/acs.chemmater.3c01260.

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Publication Details

Type

Article

Year

2023

Authors

6

Datasets

0

Total Files

0

Language

English

Journal

Chemistry of Materials

DOI

10.1021/acs.chemmater.3c01260

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